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2 article(s) from Wiles, Charlotte

Translation of microwave methodology to continuous flow for the efficient synthesis of diaryl ethers via a base-mediated S_NAr reaction

Charlotte Wiles and
Paul Watts

Beilstein J. Org. Chem. 2011, 7, 1360–1371, doi:10.3762/bjoc.7.160

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Graphical Abstract

Figure 1: Illustration of synthetically interesting diaryl ethers.

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Scheme 1: Illustration of the model reaction used to compare the enabling technologies of microwave and micro...

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Scheme 2: Illustration of the model reaction used to benchmark Labtrix S1 against batch and stopped-flow micr...

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Figure 2: Photograph illustrating Labtrix^® S1, the automated microreactor development apparatus from Chemtrix...

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Figure 3: Schematic illustrating the 10 µL reactor manifold used for the S_NAr reactions described herein (322...

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Figure 4: Schematic illustration of the reactor manifold used to evaluate the continuous-flow synthesis of 2-...

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Figure 5: Comparison of the results obtained in Labtrix^® S1 with reported data generated in a microwave synth...

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Figure 6: Screen shot from the Labtrix^® S1 control software illustrating the system file that enables the use...

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Figure 7: Summary of the results obtained for the organic base screen towards the S_NAr reaction between DCNB (...

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Figure 8: Illustration of the substituent effect on the synthesis of diaryl ethers under continuous flow (res...

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Figure 9: Schematic illustrating the mixing of immiscible reagent streams in a microfluidic channel, whereby ...

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Figure 10: Comparison of base effect on the synthesis of 2-chloro-1-(4-methoxyphenoxy)-4-nitrobenzene (7) (res...

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Figure 11: Graphical representation of an automated flow reaction for equilibration and screening of reactor t...

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Full Research Paper

Published 04 Oct 2011

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The development and evaluation of a continuous flow process for the lipase- mediated oxidation of alkenes

Charlotte Wiles,
Marcus J. Hammond and
Paul Watts

Beilstein J. Org. Chem. 2009, 5, No. 27, doi:10.3762/bjoc.5.27

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Scheme 1: Illustration of the chemo-enzymatic epoxidation of an alkene; involving the biocatalytic perhydroly...

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Scheme 2: Illustration of the chemo-enzymatic epoxidation of 1-methylcyclohexene (6) to 1-methylcyclohexene o...

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Scheme 3: Model reaction used to compare the continuous flow epoxidation strategy with the conventional batch...

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Figure 1: Schematic of the reaction set-up used to evaluate the continuous flow chemo-enzymatic epoxidation o...

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Figure 2: Graph illustrating the effect of flow rate (hence residence time) on the conversion of 1-methylcycl...

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Figure 3: Graph illustrating the effect of (a) flow rate and (b) residence time on the conversion of 1-methyl...

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Figure 4: Graph illustrating the effect of oxidant stoichiometry on the conversion of 1-methylcyclohexene (6)...

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Figure 5: Illustration of the enzyme 4 stability to H₂O₂ (2) for the conversion of 1-methylcyclohexene (6) to...

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Scheme 4: Illustration of the reaction products obtained when conducting the continuous flow epoxidation of c...

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Full Research Paper

Published 02 Jun 2009

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Translation of microwave methodology to continuous flow for the efficient synthesis of diaryl ethers via a base-mediated SNAr reaction

The development and evaluation of a continuous flow process for the lipase- mediated oxidation of alkenes

Translation of microwave methodology to continuous flow for the efficient synthesis of diaryl ethers via a base-mediated S_NAr reaction